Refer to page #7, #9, #36





Recovery (%) n = 4, average values
Additive amount 0.05 μg/g 0.5 μg/g
Oxytetracycline 85.6 90.1
Tetracycline 90.7 90.0
Chlortetracycline 94.7 96.4
Additive amount 0.25 μg/g 0.5 μg/g
Chloramphenicol 77.9 80.5

Column :Wakopak@Navi C18-5(4.6 mm×150 mm)
Eluent :CH3CN/10 mmol/L Oxalic acid=20/80(v/v)
Flow Rate :1.0 mL/min. at35℃
Detection :Tetracyclines UV 370 nm
Injection Volume :100 μL
Sample :1)Oxytetracycline(OTC)
      2)Tetracycline(TC)
      3)Chlortetracycline(CTC)
      4)Chloramphenicol(CP)



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