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HPLCアプリケーションデータ
Analysis of Pesticides

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Analysis of Pesticides, Pesticide Mixture Standard Solution GF-1(LC/MS/MS) (PDF file=140KB)

Column Wakopak® Wakosil-II 3C18HG, φ2.0mm×150mm




　
Eluent A ； 5 mmol/l Ammonium Acetate
B ； Methanol
0-1min. B conc. 15-40%, 1-3.5min. B conc. 40%, 3.5-6min. B conc. 40-50%,
6-8min. B conc. 50-55%, 8-17.5min. B conc. 55-95%, 17.5-30min. B conc. 95%
Flow rate 0.2ml/min
Detector LC/MS/MS
Injection 0.1μg/ml, 3μl
Sample 1.　 Thiamethoxam
2. 　Imidacloprid
3. 　Clothianidin
4. 　Acetamiprid
5. 　Flazasulfuron
6. 　Halosulfuron-methyl
7. 　Simazine(CAT)
8. 　Cyclosulfamuron
9.　 Metalaxyl
10. 　Azoxystrobin
11. 　Siduron
12. 　Boscalid
13. 　Flutolanil
14. 　Isoprothiolane
15. 　Mepronil
16. 　Propyzamide
17.　 Cyproconazole
18. 　Cafenstrole
19. 　Fenitrothion(MEP)
20. 　Triflumizole Metabolite
21. 　Tetraconazole
22. 　Simeconazole
23. 　Iprodione
24. 　Tebuconazole
25.　 Propiconazole
26. 　Diazinon
27. 　Butamifos
28. 　Isoxathion
29. 　Pencycuron
30. 　Difenoconazole
31. 　Terbucarb(MBPMC)
32. 　Dithiopyr
33. 　Triflumizole
34.　 Oxaziclomefone
35. 　Pyributicarb
36. 　Pendimethalin
37. 　Cafenstrole-decarbamoyl
[3-(2,4,6-Trimethylphenylsulfonyl)-1,2,4-triazole]
38. 　Triclopyr
39. 　Mecoprop(MCPP)
40. 　Thifluzamide
41. 　Tebufenozide
Category Analysis of Pesticides

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Analysis of Methamidophos and Acephate (PDF file=50KB)

Column Wakosil-II5C18 RS, 4.6mm I.D. x 150mm 　
Eluent CH3CN/H2O=5/95(v/v)
Flow rate 1.0ml/min, at R.T.
Detector UV 220nm, 0.01AUFS.
Injection 20ul, 0.01mg/ml (H2O)
Sample
  1. Methamidophos
  2. Acephate
Category Pesticides

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Analysis of Pessticides, N-Methylcarbamate (PDF file=52KB)

Column Wakosil-II5C18-100, 4.6mm I.D. x 150mm 　
Eluent A) H2O
B) CH3OH
0-10min. B conc. 18%,
10-40min. B conc. 18-70%,
40-43min. B conc. 70-90%,
43min. B conc. 90%
Flow rate 0.8mL/min, at 50C
Detector FL (Ex 340nm, Em 445nm)
Injection 20uL
Sample 1.　 Butoxycarboxim
2. 　Methomyl
3. 　Butocarboxim
4. 　Metolcarb
6. 　Bendiocarb
7. 　XMC
8. 　Pirimicarb
9. 　Trimethacarb
10. 　Methiocarb 0.2ppm (50% CH3OH)
Category Pesticide

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Analysis of Pesticide (PDF file=52KB)

Column Wakosil -Ⅱ 5C18 AR, 4.6mm I.D.×150mm 　
Eluent H2O/CH3CN=30/70（v/v）
Flow rate 1.0ml/min. at 40℃
Detector UV 225nm, 0.064AUFS
Injection 10μl
Sample
  1. Etobenzanid
  2. Pentoxazone
  3. Butachlor
  4. trans-Permethrin
  5. Ethofenprox
  6. cis-Permethrin
  7. Silafluofen10ppm（CH3CN）
Category Pesticide

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Analysis of Pesticide (PDF file=217KB)

Column Wakosil -Ⅱ 5C18 AR, 4.6mm I.D.×150mm 　
Eluent H2O/CH3CN=50/50（v/v）
Flow rate 1.0ml/min. at 40℃
Detector UV 225nm, 0.064AUFS
Injection 10μl
Sample
  1. Benfuresate
  2. Dymron
  3. Iprodione
  4. Pyrazoxyfen
  5. Tebufenozide
  6. Iprodione Metabolite
  7. Pencycuron 10ppm（CH3CN）
Category Pesticide

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Analysis of Pesticide (PDF file=192KB)

Column Wakosil -Ⅱ 5C18 AR, 4.6mm I.D.×150mm 　
Eluent A）H2O,　B）CH3CN
0-15min.B conc. 30-60%,
15-20min. B conc. 60%
Flow rate 1.0ml/min. at 40℃
Detector UV 225nm, 0.064AUFS
Injection 10μl
Sample
  1. Tricyclazole
  2. Diclomezine
  3. Carpropamid 10ppm（CH3CN）
Category Pesticide

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Analysis of Pesticides (PDF file=50KB)

Column Wakosil Agri-9, 4.6mm I.D. x 250mm 　
Eluent H3O/CH3CN=60/40(v/v)
Flow rate 1.0ml/min, at 40C
Detector UV 225nm, 0.064AUFS.
Injection 10ul, 10ppm (CH3CN)
Sample
  1. Benfuresate
  2. Dymron
  3. Iprodione
  4. Pyrazoxyfen
  5. Tebufenozide
  6. Iprodione Metabolite
  7. Pencycuron
Category Pesticides

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Analysis of Pesticides (PDF file=50KB)

Column Wakosil-II5C18 AR, 4.6mm I.D. x 150mm 　
Eluent H2O/CH3CN=55/45(v/v)
Flow rate 1.0ml/min, at 40C
Detector 1.0ml/min, at 40C
Injection 10ul, 10ppm (CH3CN)
Sample
  1. Benfuresate
  2. Dymron
  3. Iprodione
  4. Pyrazoxyfen
  5. Tebufenozine
  6. Iprodione Metabolite
  7. Pencycuron
Category Pesticides

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Analysis of Pesticides (PDF file=49KB)

Column Wakosil Agri-9, 4.6mm I.D. x 250mm 　
Eluent H2O/CH3CN=45/55(v/v)
Flow rate 1.0ml/min, at 40C
Detector UV 225nm, 0.064AUFS.
Injection 10ul, 10ppm (CH3CN)
Sample
  1. Etobenzanid
  2. Butachlor
  3. Pentoxazone
  4. Ethofenprox
  5. trans-Permethrin
  6. cis-Permethrin
  7. Silafluofen
Category Pesticides

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Analysis of Pesticides (PDF file=49KB)

Column Wakosil-II5C18 AR, 4.6mm I.D x 150mm 　
Eluent H2O/CH3CN=30/70(v/v)
Flow rate 1.0ml/min, at 40C
Detector UV 225nm, 0.064AUFS.
Injection 10ul, 10ppm (CH3CN)
Sample
  1. Etobenzanid
  2. Pentoxazone
  3. Butachlor
  4. trans-Permethrin
  5. Ethofenprox
  6. cis-Permethrin
  7. Silafluofen
Category Pesticides

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Analysis of Pesticides (PDF file=49KB)

Column Wakosil Agri-9, 4.6mm I.D. x 250mm 　
Eluent H2O/CH3CN=60/40(v/v)
Flow rate 1.0ml/min, at 50C
Detector UV 225nm, 0.064AUFS.
Injection 10ul, 10ppm (CH3CN)
Sample
  1. Benfuresate
  2. Dymron
  3. Iprodione
  4. Pyrazoxyfen
  5. Tebufenozide
  6. Iprodione Metabolite
  7. Pencycuron
Category Pesticides

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